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Born and raised in Adelaide, South Australia, Oliphant graduated from the University of Adelaide in 1922. He was awarded an 1851 Exhibition Scholarship in 1927 on the strength of the research he had done on mercury, and went to England, where he studied under Sir Ernest Rutherford at the University of Cambridge's Cavendish Laboratory. There, he used a particle accelerator to fire heavy hydrogen nuclei (deuterons) at various targets. He discovered the respective nuclei of helium-3 (helions) and of tritium (tritons). He also discovered that when they reacted with each other, the particles that were released had far more energy than they started with. Energy had been liberated from inside the nucleus, and he realised that this was a result of nuclear fusion.

Oliphant left the Cavendish Laboratory in 1937 to become the Poynting Professor of Physics at the University of Birmingham. He attempted to build a 60-inch (150 cm) cyclotron at the university, but its completion was postponed by the outbreak of the Second World War in Europe in 1939. He became involved with the development of radar, heading a group at the University of Birmingham that included John Randall and Harry Boo

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